Indentation + User defined profile Max load : 1000.00 mN Loading rate : 6000.00 mN/min Pause : 60.0 s Max load : 20.00 mN Loading rate : 6000.00 mN/min Pause : 60.0 s Max load : 1000.00 mN Loading rate : 6000.00 mN/min Pause : 60.0 s Max load : 20.00 mN Loading rate : 6000.00 mN/min Pause : 60.0 s Max load : 1000.00 mN Loading rate : 6000.00 mN/min Pause : 60.0 s Max load : 0.00 mN Loading rate : 6000.00 mN/min Date : 13-05-06 Time : 07:36:50 Method : Oliver & Pharr Cycle n? 1 + Main results Hv= 3.4421 Vickers H= 33.767 MPa E= 1.4413 GPa + Hypothesis Poisson= 0.30 + Additional results Pm= 1008.55 mN Hm= 12887.20 nm S= 0.3068 mN/nm Hc= 9599.39 nm Ht= 9599.39 nm H0= 6187.10 nm m= 2.09 Epsilon= 1.00 Ac= 29867882496.00 nm? Cycle n? 2 + Main results Hv= 3.4211 Vickers H= 33.561 MPa E= 1.4653 GPa + Hypothesis Poisson= 0.30 + Additional results Pm= 1008.79 mN Hm= 12885.93 nm S= 0.3128 mN/nm Hc= 9661.17 nm Ht= 9661.17 nm H0= 6480.89 nm m= 2.03 Epsilon= 1.00 Ac= 30058223616.00 nm? Cycle n? 3 + Main results Hv= 3.4124 Vickers H= 33.476 MPa E= 1.4719 GPa + Hypothesis Poisson= 0.30 + Additional results Pm= 1007.51 mN Hm= 12877.91 nm S= 0.3144 mN/nm Hc= 9673.62 nm Ht= 9673.62 nm H0= 6552.00 nm m= 2.01 Epsilon= 1.00 Ac= 30096578560.00 nm? Measured values Time (s) Pd (nm) Fn (mN) 0 0 0 0 0 0.3647 86.255 0.7024 0 0 0.7294 164.2919 1.124 0 0 1.094 236.6828 1.3274 0 0 1.4587 309.258 1.8972 0 0 1.8234 377.0125 2.4076 0 0 2.1881 442.6065 3.176 0 0 2.5527 500.7004 3.6674 0 0 2.9174 553.5837 4.4626 0 0 3.2821 601.7104 5.6538 0 0 3.6468 636.7488 6.9769 0 0 4.0114 675.5455 7.7118 0 0 4.3761 708.712 9.1604 0 0 4.7408 1259.6501 36.406 0 0 5.1055 1759.403 75.2061 0 0 5.4701 2118.9045 105.3588 0 0 5.8348 2587.1233 145.4694 0 0 6.1995 2932.3384 174.9829 0 0 6.5642 3375.5315 215.6124 0 0 6.9288 3813.5879 255.3279 0 0 7.2935 4145.0879 285.5036 0 0 7.6582 4579.2041 325.3627 0 0 8.0229 4985.8066 365.3167 0 0 8.3875 5276.834 395.1204 0 0 8.7522 5670.583 435.5015 0 0 9.1169 6057.9404 475.4386 0 0 9.4816 6339.5859 505.529 0 0 9.8462 6708.5752 545.3226 0 0 10.2109 7090.7847 585.5861 0 0 10.5756 7372.4116 615.3774 0 0 10.9403 7747.6401 655.6074 0 0 11.3049 8019.4624 684.9608 0 0 11.6696 8377.0723 725.2715 0 0 12.0343 8739.0361 765.3961 0 0 12.399 9010.1064 795.2042 0 0 12.7636 9378.4443 835.2708 0 0 13.1283 9736.0029 875.255 0 0 13.493 10006.3916 905.4094 0 0 13.8577 10372.6416 945.0656 0 0 14.2223 10732.5 985.3915 0 0 14.587 10986.8887 1011.3177 0 0 14.9517 11152.9268 1009.6072 0 0 15.3163 11267.9229 1009.5691 0 0 15.681 11339.4424 1009.4165 0 0 16.0457 11415.2754 1009.5187 0 0 16.4104 11468.5176 1009.5782 0 0 16.7751 11532.3018 1009.3813 0 0 17.1397 11592.5908 1009.5279 0 0 17.5044 11628.3379 1009.6652 0 0 17.8691 11672.79 1009.5752 0 0 18.2338 11711.1563 1009.2639 0 0 18.5984 11743.0244 1009.6362 0 0 18.9631 11779.874 1009.5844 0 0 19.3278 11816.6611 1009.8071 0 0 19.6925 11839.4385 1009.4103 0 0 20.0571 11872.4277 1009.8528 0 0 20.4218 11897.6064 1009.5263 0 0 20.7865 11917.0146 1009.4027 0 0 21.1511 11943.416 1009.2516 0 0 21.5158 11964.3174 1009.6021 0 0 21.8805 11984.9795 1009.36 0 0 22.2452 12012.5771 1009.5934 0 0 22.6098 12029.9707 1009.444 0 0 22.9745 12048.5898 1009.7354 0 0 23.3392 12062.4941 1009.3158 0 0 23.7039 12074.2559 1009.5889 0 0 24.0686 12096.0547 1009.65 0 0 24.4332 12117.5986 1009.7827 0 0 24.7979 12130.6475 1009.5721 0 0 25.1626 12146.2617 1009.5355 0 0 25.5273 12156.7539 1009.5279 0 0 25.8919 12172.3643 1009.4027 0 0 26.2566 12175.0205 1009.2075 0 0 26.6213 12195.1641 1009.4805 0 0 26.986 12205.7354 1009.4547 0 0 27.3506 12217.6826 1009.5339 0 0 27.7153 12228.4629 1009.4114 0 0 28.08 12245.8848 1009.36 0 0 28.4447 12257.4131 1009.6102 0 0 28.8093 12268.3164 1009.5492 0 0 29.174 12272.875 1009.4271 0 0 29.5387 12292.5889 1009.7003 0 0 29.9034 12299.3701 1009.7141 0 0 30.268 12314.3262 1009.5676 0 0 30.6327 12317.8477 1009.6789 0 0 30.9974 12332.8145 1009.5844 0 0 31.3621 12339.6641 1009.2745 0 0 31.7267 12351.7246 1009.7797 0 0 32.0914 12352.0186 1009.5615 0 0 32.4561 12365.5049 1009.656 0 0 32.8208 12373.0205 1009.5366 0 0 33.1854 12380.3438 1009.4195 0 0 33.5501 12385.3389 1009.3158 0 0 33.9148 12390.792 1009.3729 0 0 34.2794 12401.1025 1009.3417 0 0 34.6441 12407.4727 1009.5294 0 0 35.0088 12417.0264 1009.2806 0 0 35.3735 12427.3545 1009.6072 0 0 35.7382 12437.5801 1009.6118 0 0 36.1028 12450.0039 1009.6026 0 0 36.4675 12454.1875 1009.3707 0 0 36.8322 12458.7139 1009.4073 0 0 37.1968 12470.1182 1009.6865 0 0 37.5615 12478.4609 1009.5767 0 0 37.9262 12485.4502 1009.4702 0 0 38.2909 12483.8701 1009.8712 0 0 38.6556 12494.166 1009.4729 0 0 39.0202 12498.8252 1009.5533 0 0 39.3849 12506.7314 1009.5996 0 0 39.7496 12511.6787 1009.7659 0 0 40.1143 12515.9619 1009.1278 0 0 40.4789 12527.042 1009.3798 0 0 40.8436 12531.3311 1009.6789 0 0 41.2083 12537.876 1009.6026 0 0 41.573 12542.8271 1009.4669 0 0 41.9376 12549.7725 1009.656 0 0 42.3023 12558.9619 1009.5157 0 0 42.667 12559.0596 1009.4974 0 0 43.0317 12570.2031 1009.6014 0 0 43.3963 12573.8262 1009.4897 0 0 43.761 12578.1016 1009.3722 0 0 44.1257 12581.6006 1009.5458 0 0 44.4904 12591.3252 1009.6484 0 0 44.855 12593.3701 1009.7217 0 0 45.2197 12599.6016 1009.5353 0 0 45.5844 12602.668 1009.511 0 0 45.9491 12612.123 1009.5263 0 0 46.3137 12610.3574 1009.2225 0 0 46.6784 12618.4102 1009.386 0 0 47.0431 12625.2598 1009.7644 0 0 47.4078 12628.6543 1009.5065 0 0 47.7724 12633.5254 1009.5187 0 0 48.1371 12639.1533 1009.592 0 0 48.5018 12641.7441 1009.5966 0 0 48.8665 12648.8125 1009.7247 0 0 49.2311 12653.6738 1009.4034 0 0 49.5958 12656.6992 1009.6729 0 0 49.9605 12663.917 1009.3372 0 0 50.3252 12668.6836 1009.566 0 0 50.6898 12670.7383 1009.4226 0 0 51.0545 12671.9141 1009.4714 0 0 51.4192 12677.5879 1009.8853 0 0 51.7839 12687.8193 1009.3982 0 0 52.1485 12682.9619 1009.3936 0 0 52.5132 12684.7822 1009.6282 0 0 52.8779 12694.8252 1009.4363 0 0 53.2425 12698.9365 1009.325 0 0 53.6072 12698.3545 1009.3966 0 0 53.9719 12704.1572 1009.4653 0 0 54.3366 12709.627 1009.5199 0 0 54.7013 12710.5928 1009.325 0 0 55.0659 12715.5547 1009.3921 0 0 55.4306 12717.3682 1009.4865 0 0 55.7953 12720.0771 1009.4897 0 0 56.16 12732.2568 1009.3768 0 0 56.5246 12732.4531 1009.4794 0 0 56.8893 12736.9248 1009.5752 0 0 57.254 12737.168 1009.3372 0 0 57.6187 12745.3311 1009.759 0 0 57.9833 12747.9688 1009.5844 0 0 58.348 12750.3662 1009.4805 0 0 58.7127 12753.667 1009.4794 0 0 59.0774 12757.0859 1009.3951 0 0 59.442 12758.9043 1009.376 0 0 59.8067 12762.3506 1009.4714 0 0 60.1714 12769.9023 1009.7552 0 0 60.5361 12778.7119 1009.6412 0 0 60.9007 12776.8545 1009.4211 0 0 61.2654 12781.7656 1009.3631 0 0 61.6301 12788.1289 1009.2415 0 0 61.9948 12789.8711 1009.743 0 0 62.3594 12789.6055 1009.5599 0 0 62.7241 12788.5244 1009.4073 0 0 63.0888 12802.9023 1009.3112 0 0 63.4535 12803.4629 1009.3478 0 0 63.8181 12800.2803 1009.5287 0 0 64.1828 12802.0947 1009.3722 0 0 64.5475 12808.1279 1009.3367 0 0 64.9122 12807.8428 1009.6316 0 0 65.2768 12813.6602 1009.2593 0 0 65.6415 12813.1113 1009.4935 0 0 66.0062 12816.1309 1009.4684 0 0 66.3708 12816.7383 1009.5873 0 0 66.7355 12822.8271 1009.5067 0 0 67.1002 12825.9707 1009.5905 0 0 67.4649 12830.8096 1009.4531 0 0 67.8296 12830.8633 1009.4672 0 0 68.1942 12829.4414 1009.4241 0 0 68.5589 12836.9248 1009.5324 0 0 68.9236 12842.0332 1009.281 0 0 69.2883 12838.7764 1009.9124 0 0 69.6529 12846.417 1009.36 0 0 70.0176 12848.2637 1009.5468 0 0 70.3823 12855.0459 1009.4165 0 0 70.747 12859.4063 1009.1643 0 0 71.1116 12863.2168 1009.6973 0 0 71.4763 12863.9697 1009.3158 0 0 71.841 12868.7422 1009.3311 0 0 72.2057 12872.7188 1009.5706 0 0 72.5703 12873.1445 1009.685 0 0 72.935 12873.4766 1009.5681 0 0 73.2997 12877.4014 1009.511 0 0 73.6644 12881.4756 1009.4042 0 0 74.029 12886.4932 1009.686 0 0 74.3937 12890.1416 1009.7675 0 0 74.7584 12862.4961 990.1508 0 0 75.1231 12767.6885 955.2967 0 0 75.4877 12647.3721 915.9273 0 0 75.8524 12548.2988 881.6406 0 0 76.2171 12429.4609 844.7563 0 0 76.5817 12299.3232 805.2689 0 0 76.9464 12177.4688 771.9893 0 0 77.3111 12043.002 735.2019 0 0 77.6758 11903.6123 695.2285 0 0 78.0405 11766.0869 662.1515 0 0 78.4051 11617.1143 625.2286 0 0 78.7698 11440.7891 585.1421 0 0 79.1345 11298.4434 553.0873 0 0 79.4992 11117.9541 515.2031 0 0 79.8638 10928.376 480.0391 0 0 80.2285 10750.3984 443.7338 0 0 80.5932 10530.501 404.912 0 0 80.9579 10320.917 370.3813 0 0 81.3225 10087.0283 333.9563 0 0 81.6872 9827.4434 297.5566 0 0 82.0519 9552.5576 261.212 0 0 82.4165 9249.959 224.7072 0 0 82.7812 8877.7852 185.1299 0 0 83.1459 8524.3652 151.6236 0 0 83.5106 8079.5767 115.1579 0 0 83.8753 7493.396 75.3297 0 0 84.2399 6893.7871 42.7805 0 0 84.6046 6003.1602 8.7204 0 0 84.9693 5619.2441 9.1842 0 0 85.334 5451.2764 9.5292 0 0 85.6986 5307.8296 9.0027 0 0 86.0633 5200.9736 9.5415 0 0 86.428 5112.0723 9.2808 0 0 86.7927 5031.3901 8.995 0 0 87.1573 4968.6553 9.3143 0 0 87.522 4917.3369 9.2273 0 0 87.8867 4858.8408 9.0332 0 0 88.2514 4824.1646 9.3178 0 0 88.616 4785.3159 9.3277 0 0 88.9807 4737.7544 9.108 0 0 89.3454 4713.2871 9.2882 0 0 89.7101 4678.1353 9.346 0 0 90.0747 4644 8.9752 0 0 90.4394 4619.6641 9.0116 0 0 90.8041 4593.3994 9.5321 0 0 91.1688 4567.8501 9.0866 0 0 91.5334 4549.5938 9.3282 0 0 9...
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